Halogenation of organic compounds using continuous flow and microreactor technology
Abstract The halogenation of organic substrates is one the most important transformations in organic synthesis. The most straightforward, inexpensive and atom economic halogenations involve the use of elemental halogens (X2)…
Continuous handling of reactions forming solids
We selected two reactions to assess the ability of the CSTR cascade to handle the formation of solids: (i) reaction of glyoxal with cyclohexylamine to form N,N′-dicyclohexylethylenediimine that is insoluble in…
General procedure for solid-forming reactions in the CSTR cascade
The scheme of the setup for continuous handling of solid-forming reactions in the CSTR cascade is shown in Fig. S2 (see the ESI†). The reagents for the reactions were dissolved…
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Residence time distribution (RTD) characterization
The RTD profiles of the CSTR cascade were obtained using the pulse injection method (Fig. 2). The carrier phase was deionized (DI) water, and the tracer was methylene blue. In-line…
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